pyeunicam sp3 300 spectrometer (Pye Unicam Ltd)
86
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Pye Unicam Ltd
pyeunicam sp3 300 spectrometer
Pyeunicam Sp3 300 Spectrometer, supplied by Pye Unicam Ltd, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/300s/instrument+pye+sp300+unicam/10__23975_slash_bjvetr__2031__175861-16-11-11
Average 86 stars, based on 1 article reviews
Pyeunicam Sp3 300 Spectrometer, supplied by Pye Unicam Ltd, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/300s/instrument+pye+sp300+unicam/10__23975_slash_bjvetr__2031__175861-16-11-11
Average 86 stars, based on 1 article reviews
pyeunicam sp3 300 spectrometer - by Bioz Stars,
2026-11
86/100 stars
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Adhesive:Article Title: Reactions of Ru(CO)ClH(C5H5N)(PPh3)2 with 1-alkynes Article Snippet: Ru(CO)ClH(C,H,N)(PPh,), reacts with an equivalent of a monosubstituted alkyne in dichloromethane to give alkenyl derivative Ru(CO)Cl((E)HC=CHR)(C,H,N)(PPh,), (R = II-C3H7, n-GH,,, n-CsHr,, CMe,, Ph, COOMe, COOEt), resulting from a &-insertion of the alkyne into the Ru-H bond.. The reaction of the ruthenium hydride with an excess of an activated alkyne HGCCOOR(R=Me, Et) in methanol under reflux yields the bis-insertion derivative Ru(CO)Cl[ROkC=CHCH=CHCOOR](PPh,), (R = Me, Et). Article Title: Isolation of Transmetalation Intermediates in the Stille Cross-Coupling Reaction of Stannanes: Synthesis of Palladacycles, Ligand Substitution, and Insertion Reactions Article Snippet: A strategy based on a Stille cross-coupling reaction of organostannanes interrupted at the reductive elimination step has been applied to the synthesis of oxaand azapalladacycles with the general formula cis-[PdArR(L),] .. The synthesis of oxapalladacycles was achieved under mild conditions by reaction of 2-iodoor 2-bromophenyloxymethylstannanes with [Pd(PPh,),].. The synthesis of an aza analogue was similarly carried out from the corresponding 2-iodoaniline derivative. Article Title: Design and synthesis of new polyphosphorylated upper-rim modified calix[4]arenes as potential and selective chelating agents of uranyl ion Article Snippet: New upper-rim polyphosphorylated calix[4]arenes were designed for decorporation of uranium in case of nuclear contamination.. A ligand system containing four preorganized 1-hydroxymethylene-1,1-bisphosphonic acid moieties anchored onto a calix[4]arene platform has been developed.. Three calix[4]arene-bisphosphonates were efficiently prepared in multi-step syntheses with a variable carbon chain length between the bisphosphonate and the calix[4]arene. Article Title: Novel incorporation of charged hydroxyapatite nanoparticles into resin adhesive. Article Snippet: 2-Ethanol (99%) and dimethylsulfoxide (DMSO) were obtained from Sigma-Aldrich 3-The Resin adhesive (Palfique Bond) was obtained from Tokuyama Dental Co. 4- Fourier Transform Infrared Spectroscopy (FTIR): Article Title: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands. Molecular and supramolecular structures of [R2Sn(OArCHNNCSNH2)], where R = Me, Ph and Ar = C6H4, C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CHNNCSNH2}]·OH2 Article Snippet: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands.. Molecular and supramolecular structures of [R2Sn(OArCH N–N CSNH2)], where R = Me, Ph and Ar = – C6H4, –C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CH N–N CSNH2}]·OH2† Moumita Sen Sarma1, Shibnath Mazumder2, Debabrata Ghosh2, Abhijit Roy1*, Andrew Duthie3 and Edward R. T. Tiekink4* Article Title: Synthesis of butenynylruthenium complexes from hydrido, alkenyl, or alkynyl complexes Article Snippet: The reaction of Ru(CO)ClH(PPh3)3 with 1 -alkynes in 1,2-dichloroethane under reflux conditions provides the coordinatively unsaturated butenynyl complexes rRu(C(C~CR)=CHR)(CO)Cl(PPh3)27 in good yield.. These and related butenynyl complexes were also prepared by starting from the corresponding alkenylor alkynylruthenium complexes.. Hydrogenolysis of [Ru{C(C~CPh)=CHPhj(CO)Cl(PPh3)27 in the presence of pyridine gave (Z)-1,4-diphenylbutenyne and Ru(C0)ClH(PY) (PPh3)z. Fourier Transform Infrared Spectroscopy:Article Title: Reactions of Ru(CO)ClH(C5H5N)(PPh3)2 with 1-alkynes Article Snippet: Ru(CO)ClH(C,H,N)(PPh,), reacts with an equivalent of a monosubstituted alkyne in dichloromethane to give alkenyl derivative Ru(CO)Cl((E)HC=CHR)(C,H,N)(PPh,), (R = II-C3H7, n-GH,,, n-CsHr,, CMe,, Ph, COOMe, COOEt), resulting from a &-insertion of the alkyne into the Ru-H bond.. The reaction of the ruthenium hydride with an excess of an activated alkyne HGCCOOR(R=Me, Et) in methanol under reflux yields the bis-insertion derivative Ru(CO)Cl[ROkC=CHCH=CHCOOR](PPh,), (R = Me, Et). Article Title: Isolation of Transmetalation Intermediates in the Stille Cross-Coupling Reaction of Stannanes: Synthesis of Palladacycles, Ligand Substitution, and Insertion Reactions Article Snippet: A strategy based on a Stille cross-coupling reaction of organostannanes interrupted at the reductive elimination step has been applied to the synthesis of oxaand azapalladacycles with the general formula cis-[PdArR(L),] .. The synthesis of oxapalladacycles was achieved under mild conditions by reaction of 2-iodoor 2-bromophenyloxymethylstannanes with [Pd(PPh,),].. The synthesis of an aza analogue was similarly carried out from the corresponding 2-iodoaniline derivative. Article Title: Design and synthesis of new polyphosphorylated upper-rim modified calix[4]arenes as potential and selective chelating agents of uranyl ion Article Snippet: New upper-rim polyphosphorylated calix[4]arenes were designed for decorporation of uranium in case of nuclear contamination.. A ligand system containing four preorganized 1-hydroxymethylene-1,1-bisphosphonic acid moieties anchored onto a calix[4]arene platform has been developed.. Three calix[4]arene-bisphosphonates were efficiently prepared in multi-step syntheses with a variable carbon chain length between the bisphosphonate and the calix[4]arene. Article Title: Novel incorporation of charged hydroxyapatite nanoparticles into resin adhesive. Article Snippet: 2-Ethanol (99%) and dimethylsulfoxide (DMSO) were obtained from Sigma-Aldrich 3-The Resin adhesive (Palfique Bond) was obtained from Tokuyama Dental Co. 4- Fourier Transform Infrared Spectroscopy (FTIR): Article Title: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands. Molecular and supramolecular structures of [R2Sn(OArCHNNCSNH2)], where R = Me, Ph and Ar = C6H4, C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CHNNCSNH2}]·OH2 Article Snippet: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands.. Molecular and supramolecular structures of [R2Sn(OArCH N–N CSNH2)], where R = Me, Ph and Ar = – C6H4, –C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CH N–N CSNH2}]·OH2† Moumita Sen Sarma1, Shibnath Mazumder2, Debabrata Ghosh2, Abhijit Roy1*, Andrew Duthie3 and Edward R. T. Tiekink4* Article Title: Synthesis of butenynylruthenium complexes from hydrido, alkenyl, or alkynyl complexes Article Snippet: The reaction of Ru(CO)ClH(PPh3)3 with 1 -alkynes in 1,2-dichloroethane under reflux conditions provides the coordinatively unsaturated butenynyl complexes rRu(C(C~CR)=CHR)(CO)Cl(PPh3)27 in good yield.. These and related butenynyl complexes were also prepared by starting from the corresponding alkenylor alkynylruthenium complexes.. Hydrogenolysis of [Ru{C(C~CPh)=CHPhj(CO)Cl(PPh3)27 in the presence of pyridine gave (Z)-1,4-diphenylbutenyne and Ru(C0)ClH(PY) (PPh3)z. Spectroscopy:Article Title: Reactions of Ru(CO)ClH(C5H5N)(PPh3)2 with 1-alkynes Article Snippet: Ru(CO)ClH(C,H,N)(PPh,), reacts with an equivalent of a monosubstituted alkyne in dichloromethane to give alkenyl derivative Ru(CO)Cl((E)HC=CHR)(C,H,N)(PPh,), (R = II-C3H7, n-GH,,, n-CsHr,, CMe,, Ph, COOMe, COOEt), resulting from a &-insertion of the alkyne into the Ru-H bond.. The reaction of the ruthenium hydride with an excess of an activated alkyne HGCCOOR(R=Me, Et) in methanol under reflux yields the bis-insertion derivative Ru(CO)Cl[ROkC=CHCH=CHCOOR](PPh,), (R = Me, Et). Article Title: Isolation of Transmetalation Intermediates in the Stille Cross-Coupling Reaction of Stannanes: Synthesis of Palladacycles, Ligand Substitution, and Insertion Reactions Article Snippet: A strategy based on a Stille cross-coupling reaction of organostannanes interrupted at the reductive elimination step has been applied to the synthesis of oxaand azapalladacycles with the general formula cis-[PdArR(L),] .. The synthesis of oxapalladacycles was achieved under mild conditions by reaction of 2-iodoor 2-bromophenyloxymethylstannanes with [Pd(PPh,),].. The synthesis of an aza analogue was similarly carried out from the corresponding 2-iodoaniline derivative. Article Title: Design and synthesis of new polyphosphorylated upper-rim modified calix[4]arenes as potential and selective chelating agents of uranyl ion Article Snippet: New upper-rim polyphosphorylated calix[4]arenes were designed for decorporation of uranium in case of nuclear contamination.. A ligand system containing four preorganized 1-hydroxymethylene-1,1-bisphosphonic acid moieties anchored onto a calix[4]arene platform has been developed.. Three calix[4]arene-bisphosphonates were efficiently prepared in multi-step syntheses with a variable carbon chain length between the bisphosphonate and the calix[4]arene. Article Title: Novel incorporation of charged hydroxyapatite nanoparticles into resin adhesive. Article Snippet: 2-Ethanol (99%) and dimethylsulfoxide (DMSO) were obtained from Sigma-Aldrich 3-The Resin adhesive (Palfique Bond) was obtained from Tokuyama Dental Co. 4- Fourier Transform Infrared Spectroscopy (FTIR): Article Title: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands. Molecular and supramolecular structures of [R2Sn(OArCHNNCSNH2)], where R = Me, Ph and Ar = C6H4, C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CHNNCSNH2}]·OH2 Article Snippet: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands.. Molecular and supramolecular structures of [R2Sn(OArCH N–N CSNH2)], where R = Me, Ph and Ar = – C6H4, –C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CH N–N CSNH2}]·OH2† Moumita Sen Sarma1, Shibnath Mazumder2, Debabrata Ghosh2, Abhijit Roy1*, Andrew Duthie3 and Edward R. T. Tiekink4* Article Title: Synthesis of butenynylruthenium complexes from hydrido, alkenyl, or alkynyl complexes Article Snippet: The reaction of Ru(CO)ClH(PPh3)3 with 1 -alkynes in 1,2-dichloroethane under reflux conditions provides the coordinatively unsaturated butenynyl complexes rRu(C(C~CR)=CHR)(CO)Cl(PPh3)27 in good yield.. These and related butenynyl complexes were also prepared by starting from the corresponding alkenylor alkynylruthenium complexes.. Hydrogenolysis of [Ru{C(C~CPh)=CHPhj(CO)Cl(PPh3)27 in the presence of pyridine gave (Z)-1,4-diphenylbutenyne and Ru(C0)ClH(PY) (PPh3)z. Spectrophotometry:Article Title: Reactions of Ru(CO)ClH(C5H5N)(PPh3)2 with 1-alkynes Article Snippet: Ru(CO)ClH(C,H,N)(PPh,), reacts with an equivalent of a monosubstituted alkyne in dichloromethane to give alkenyl derivative Ru(CO)Cl((E)HC=CHR)(C,H,N)(PPh,), (R = II-C3H7, n-GH,,, n-CsHr,, CMe,, Ph, COOMe, COOEt), resulting from a &-insertion of the alkyne into the Ru-H bond.. The reaction of the ruthenium hydride with an excess of an activated alkyne HGCCOOR(R=Me, Et) in methanol under reflux yields the bis-insertion derivative Ru(CO)Cl[ROkC=CHCH=CHCOOR](PPh,), (R = Me, Et). Article Title: Isolation of Transmetalation Intermediates in the Stille Cross-Coupling Reaction of Stannanes: Synthesis of Palladacycles, Ligand Substitution, and Insertion Reactions Article Snippet: A strategy based on a Stille cross-coupling reaction of organostannanes interrupted at the reductive elimination step has been applied to the synthesis of oxaand azapalladacycles with the general formula cis-[PdArR(L),] .. The synthesis of oxapalladacycles was achieved under mild conditions by reaction of 2-iodoor 2-bromophenyloxymethylstannanes with [Pd(PPh,),].. The synthesis of an aza analogue was similarly carried out from the corresponding 2-iodoaniline derivative. Article Title: Design and synthesis of new polyphosphorylated upper-rim modified calix[4]arenes as potential and selective chelating agents of uranyl ion Article Snippet: New upper-rim polyphosphorylated calix[4]arenes were designed for decorporation of uranium in case of nuclear contamination.. A ligand system containing four preorganized 1-hydroxymethylene-1,1-bisphosphonic acid moieties anchored onto a calix[4]arene platform has been developed.. Three calix[4]arene-bisphosphonates were efficiently prepared in multi-step syntheses with a variable carbon chain length between the bisphosphonate and the calix[4]arene. Article Title: Novel incorporation of charged hydroxyapatite nanoparticles into resin adhesive. Article Snippet: 2-Ethanol (99%) and dimethylsulfoxide (DMSO) were obtained from Sigma-Aldrich 3-The Resin adhesive (Palfique Bond) was obtained from Tokuyama Dental Co. 4- Fourier Transform Infrared Spectroscopy (FTIR): Article Title: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands. Molecular and supramolecular structures of [R2Sn(OArCHNNCSNH2)], where R = Me, Ph and Ar = C6H4, C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CHNNCSNH2}]·OH2 Article Snippet: Synthesis, spectroscopic characterization and biocidal activity of some diorganotin(IV) complexes of salicylaldehydethiosemicarbazones and related ligands.. Molecular and supramolecular structures of [R2Sn(OArCH N–N CSNH2)], where R = Me, Ph and Ar = – C6H4, –C6H3(5-Br) and C6H3(5-Cl), and of [Me2Sn{OC6H3(5-Br)CH N–N CSNH2}]·OH2† Moumita Sen Sarma1, Shibnath Mazumder2, Debabrata Ghosh2, Abhijit Roy1*, Andrew Duthie3 and Edward R. T. Tiekink4* Article Title: Synthesis of butenynylruthenium complexes from hydrido, alkenyl, or alkynyl complexes Article Snippet: The reaction of Ru(CO)ClH(PPh3)3 with 1 -alkynes in 1,2-dichloroethane under reflux conditions provides the coordinatively unsaturated butenynyl complexes rRu(C(C~CR)=CHR)(CO)Cl(PPh3)27 in good yield.. These and related butenynyl complexes were also prepared by starting from the corresponding alkenylor alkynylruthenium complexes.. Hydrogenolysis of [Ru{C(C~CPh)=CHPhj(CO)Cl(PPh3)27 in the presence of pyridine gave (Z)-1,4-diphenylbutenyne and Ru(C0)ClH(PY) (PPh3)z. |